Macrakis however gives an even earlier source for the vinegar and alum recipe, well before Wikipedia: a New York Times article from 1965, in which it’s reported that the United States Department of Agriculture recommends parents encourage their kids to eat more eggs by teaching them to write secret messages on the inside using a ‘magic ink’ made of vinegar and alum.
No doubt building on the popularity of ‘60s spy toys, they told kids to mix one ounce of alum with one cup of vinegar, then use the colorless magic ink to write a message on the shell of an uncooked egg. Once it was dry, one only had to boil the egg for 15 minutes, and—so the USDA promised—whatever secret was written on the shell would show up inside on the white of the boiled egg.
I have found a few leads that may be the USDA’s ultimate source, some dating back to the turn of the 20th century, and I’m sure there are others as well. All of these sources are missing the oak gall and none of them mention della Porta. How the one dropped out and the other dropped in is still a mystery…
For now, here are Africanus’ and della Porta’s recipes for writing messages in eggs. I also tried to reproduce Africanus’ version, with and without oak gall (well, a tannin anyway). It didn’t work.
Julius Africanus’ recipe for leaving a secret message in an egg
“To make inscriptions on eggs. From Africanus.
“Grind up oak gall and alum with vinegar until it reaches the thickness of black ink. Use it to write whatever you want on the egg. Once the writing has dried in the sun, place the egg into a sharp brine. Once it has dried, boil it, and when you have peeled it, you will find the inscription.
“If you coat the egg all over with wax and inscribe it until the shell appears through the letters, then leave it to soak in vinegar overnight, on the next day, after removing the wax, you will find that the vinegar has made the outline of the letters transparent.”
Ὠὰ κατάγραπτα ποιῆσαι. Ἀφρικανοῦ.
Κικίδος καὶ στυπτηρίας μετὰ ὄξους τρίψας, ἕως γένηται πάχος μέλανος, ἐπίγραψον ἐξ αὐτοῦ ὃ θέλεις τῷ ὠῷ, καὶ ψυγείσης τῆς γραφῆς ἐν ἡλίῳ κατάθες τὸ ὠὸν εἰς ἅλμην δριμεῖαν, καὶ ψύξας ἕψησον, καὶ λεπίσας εὑρήσεις τὴν ἐπιγραφήν. Εἰ δὲ κηρῷ περιπλάσας τὸ ὠὸν ἐπιγράψεις ἄχρις ἂν φανῇ τὸ ἔλυτρον τοῖς γράμμασιν, εἶτα ἐάσεις ὄξει βρέχεσθαι τὴν νύκτα, τῇ ἑξῆς περιελὼν τὸν κηρόν, εὑρήσεις τῶν γραμμάτων τὸν τύπον ὑπὸ τοῦ ὄξους γενόμενον διαφανῆ.
Geoponica 14.10 (roughly 10th century, recipe originally 3rd century CE, probably)
Giambattista della Porta’s recipe for leaving a secret message in an egg
“If you want to make yellow letters appear on an egg white (it will work better when the egg is cooked): Boil an egg hard, roll it in wax, and engrave the letters on the wax with an iron point so that the marks go through. Place it into a solution of powdered alum and oak galls. Then put it into sharp vinegar and they will penetrate. And taking off the shell, you will see them on the white of the egg. Africanus instructs as follows: ‘grind oak galls and alum with vinegar, until they have the viscosity of ink. With it, inscribe whatever your want on the egg and once the writing has been dried by the sun, place the egg in sharp brine, and having dried it, cook it, peel, and you will find the inscription.’ I put it in vinegar and nothing happened, unless by ‘brine’, he meant sharp lye, what’s normally called capitellum.”
Si vis autem ut litera supra albumen videantur croceae et rectius, ubi ovum excoctum fuerit: Coque ovum donec durescat et cera obline et insculpe literas stylo, ut liturae dehiscent, imponatur in humore, id est, ex gallis cum alumine tritis. Inde acri aceto impones et eae fient pentrabiles, quas cortice, detecto videbis in albumine ovi. Africanus ita docet. Gallas et alumen cum aceto terito, donec atramenti spissitudinem habeant, ex hoc quicquid libuerit ouo inscribito, et postquam scriptum Sole desiccatum fuerit, ouum in muriam acrem demittito, et resiccatum coquito, et decorticato, et reperies inscriptionem. Ego in acetum imposui, et nihil evenit, si per muriam non intelligat acre lixiviu, vulgo capitello dictum.
Giambattista della Porta, Magia Naturalis 16.4, 1590 (English, 1658)